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http://localhost:8080/xmlui/handle/123456789/208| Title: | Preparation and Characterization of Novel disubstituted 1,3- Oxazepine tetra-one from Schiff bases reaction with 3-methylfuran-2,5-dione and 3- Phenyldihydrofuran-2,5-dione |
| Authors: | Abdul Kareem Hamad Ayfan, Rasim F. Muslim Noor Sabah Noori |
| Keywords: | 1H-NMR 13C-NMR TLC Schiff bases oxazepine-tetra-one |
| Issue Date: | 2019 |
| Publisher: | Research Journal of Pharmacy and Technology |
| Abstract: | This research includes synthesis of new heterocyclic derivatives of novel disubstituted 1,3- oxazepine-tetra-one from Schiff bases reaction with 3-methylfuran-2,5-dione and 3-phenyldihydrofuran-2,5-dione. Schiff bases [A1- A5] were synthesized by the reaction of aromatic aldehydes with primary aromatic amines, in the presence of glacial acetic acid as catalyst in absolute ethanol. The novel derivatives[A6-A10] were obtained from treatment of Schiff bases with anhydrides. The synthesized compounds were identified by TLC and via spectral methods, their (FT-IR, 1H-NMR and 13C-NMR) and measurements of some of its physical properties |
| URI: | http://localhost:8080/xmlui/handle/123456789/208 |
| ISSN: | 0974-3618 (Print) 0974-360X (Online) |
| Appears in Collections: | قسم البيئة |
Files in This Item:
| File | Description | Size | Format | |
|---|---|---|---|---|
| Kareem, Rasim and Noor 7membered.pdf | 1.38 MB | Adobe PDF | View/Open |
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