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http://localhost:8080/xmlui/handle/123456789/9280| Title: | Preparation and characterization of novel disubstituted 1,3- oxazepine-tetra-one from schiff bases reaction with 3-methylfuran-2,5-dione and 3-phenyldihydrofuran-2,5-dione |
| Authors: | Abdul Kareem Hamad Ayfan, Rasim Farraj Muslim Noor Sabah Noori |
| Keywords: | 1H-NMR 13C-NMR TLC Schiff bases oxazepine-tetra-one. |
| Issue Date: | 2019 |
| Publisher: | A and V Publications / Research Journal of Pharmacy and Technology |
| Citation: | 10 |
| Abstract: | This research includes synthesis of new heterocyclic derivatives of novel disubstituted 1,3- oxazepine-tetra-onefrom Schiff bases reaction with 3-methylfuran-2,5-dione and 3-phenyldihydrofuran-2,5-dione. Schiff bases [A1-A5] were synthesized by the reaction of aromatic aldehydes with primary aromatic amines, in the presence ofglacial acetic acid as catalyst in absolute ethanol. The novel derivatives[A6-A10] were obtained from treatment ofSchiff bases with anhydrides. The synthesized compounds were identified by TLC and via spectral methods,their (FT-IR, 1H-NMR and 13C-NMR) and measurements of some of its physical propertie |
| URI: | http://localhost:8080/xmlui/handle/123456789/9280 |
| ISSN: | 0974-3618 |
| Appears in Collections: | كلية الصيدلة |
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